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40 Pesticides out of a multi-target screening method for 300 compounds

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Application Detail (App ID: 15632)

Column: Synergi™ 4 µm Fusion-RP 80 Å, LC Column 50 x 2 mm, Ea

Part No:00B-4424-B0

Dimensions:50 x 2 mm ID

Elution Type:Gradient

Elution A:H2O + 5mM NH4formate

Elution B:CH3OH + 5mM NH4formate

Gradient Profile:

Step No.	Time (min)	Pct A	Pct B
1	0	80	20
2	11	10	90
3	23	10	90

Flow Rate:0.2 mL/min

Col. Temp: 20 °C

Detection: Mass Spectrometer (MS) @ amu (22°C)

Detector Info: SCIEX 4000 QTRAP® LC/MS/MS system, Turbo V, source with TurboIonSpray® probe
TEM = 450°C, IS= 5000V, Declustering Potential (DP) = 30V, Collision Energy (CE) = optimized for each compound
Positive polarity, Multiple Reaction Monitoring of 297 transitions (MRMs of example see table)

Information Dependent Acquisition of 3 Enhanced Product Ion spectra to confirm detected compound at CE = 20, 35, and 50V, Dynamic fill time to avoid linear ion trap saturation, Dynamic background subtraction to allow detection of co-eluting peaks, Mass spectral library searching

Note:SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, Fusion-RP 4 x 2.0mm, 10/Pk Part No.: AJ0-7556
- Holder Part No.: KJ0-4282

Analyte Details

Analyte Detail not available

Ethiofencarb-sulfone

Ethiofencarb-sulfoxide

Imidacloprid

Cinosulfurone

Propamocarb

Vamidothion

Dimethoate

Carbendazim

Thiacloprid

Desmethyl-pirimicarb

Propoxur

Carbofuran

Desmethyl-formamido-pirimicarb

Thiophanate-methyl

Thiabendazole

Ethiofencarb

Pirimicarb

Thiodicarb

Atrazine

Metalaxyl

3,4,5 Trimethacarb

Diuron

Desmedipham

Azoxystrobin

Linuron

Methiocarb

Promecarb

Iprovalicarb

Metolachlor

Diflubenzurone

Tebufenozide

Tebuconazole

Cyprodinil

Spiroxamine

Haloxyfop-methyl

Haloxyfop-etotyl

Quizalofop-ethyl

Fluazifop-P-butyl

Furathiocarb

Fenpropimorph

Ethiofencarb-sulfone