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Organochloropesticides (OCP) and Polychlorinated Biphenyls (PCB) in Milk and Milk Products by GC/ECD

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Application Detail (App ID: 17909)

Column:Zebron™ ZB-MultiResidue™-1, GC Cap. Column 30 m x 0.25 mm x 0.25 µm, Ea

Part No:7HG-G016-11

Phase:Proprietary Pesticides Phase

Dimensions:30 meters x 0.25 mm x 0.25 µm

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Products for this Application

Oven Profile:100 °C for 2 min, with 30 °C/min to 160 °C, with 2 °C/min to 170 °C, with 4 °C/min to 190°C and 10 min hold, with 10 °C/min to 220 °C and 5 min hold, with 10 °C/min to 250°C and 5 min hold

Carrier Gas:Constant Flow Hydrogen, 1.5 mL/min

Injection:Splitless :1 5 µL @ 50°C

Detection: Electron Capture (ECD) (300°C)

Note:The application was kindly provided by the MLF, Dr.-Oskar-Farny-Institute in Wangen, Germany.

Injector Gerstel-KAS3. Program: 50 °C with 12 °C/s to 300 °C, 3 min hold
Solvent Venting Purge Time: 0.15 min, Splitless Time: 1 min, Equilibration Time 0.5 min, Initial Time: 0.15 min.

Concentration: 25 ppb each for OCP + PCB, 100 ppb for Nitrofen

Analyte Details

Analyte Detail not available

alpha-HCH

Hexachlorobenzene

gamma-HCH

beta-HCH

delta-HCH

PCB 28

PCB 52

Aldrin

Heptachloro epoxide

2,4'-DDE (o,p-)

PCB 101

4,4'-DDE (p,p-)

Nitrofen

Dieldrin

2,4'-DDD (o,p-)

Endrin

4,4'-DDD (p,p-)

PCB 153

PCB 138

PCB 180

Mirex