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EPA Method 8330: Explosive Mix Using Synergi Hydro-RP

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Application Detail (App ID: 18146)

Column: Synergi™ 4 µm Hydro-RP 80 Å, LC Column 250 x 4.6 mm, Ea

Part No:00G-4375-E0

Dimensions:250 x 4.6 mm ID

Elution Type:Gradient

Elution A:Methanol

Elution B:20mM KH2PO4-pH=2.5

Gradient Profile:

Step No.	Time (min)	Pct A	Pct B
1	0	55	45
2	2	55	45
3	12	65	35
4	22	65	35

Flow Rate:1 mL/min

Col. Temp: 25 °C

Detection: UV-Vis Abs.-Variable Wave.(UV) @ 254 nm (22°C)

Note:100ul of 100ug/ml 17 component mix was diluted with 900ul of 50:50 Methanol/water

Analyte Details

Analyte Detail not available

Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX)

Hexahydro-1,3,5-trinitro-1,3,5-triazine

Picric acid

1,3,5-Trinitrobenzene (1,3,5-TNB)

Methyl-2,4,6-trinitrophenylnitramine

1,3-Dinitrobenzene (1,3-DNB)

Nitrobenzene

Nitroglycerin

2,4,6-Trinitrotoluene (2,4,6-TNT)

3,5-Dinitroaniline

4-Amino-2,6-dinitrotoluene

2-Amino-4,6-dinitrotoluene

2,6-Dinitrotoluene (2,6-DNT)

2,4-Dinitrotoluene (2,4-DNT)

Pentaerythritol tetranitrate (PETN)

2-Nitrotoluene

4-Nitrotoluene

3-Nitrotoluene