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Quantification of Organophosphorus Pesticides by QuEchERS and LC/MS/MS

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Application Detail (App ID: 20020)

Column: Synergi™ 4 µm Fusion-RP 80 Å, LC Column 50 x 2 mm, Ea

Part No:00B-4424-B0

Dimensions:50 x 2 mm ID

Elution Type:Gradient

Elution A:Add 5mL of 1M ammonium formate to 1L Water

Elution B:Add 5mL of 1M ammonium formate to 1L Methanol

Gradient Profile:

Step No.	Time (min)	Pct A	Pct B
1	-5	95	5
2	0	95	5
3	2	95	5
4	6	50	50
5	12	10	90
6	14	10	90
7	16	95	5
8	17	95	5

Flow Rate:250 mL/min

Col. Temp: 25 °C

Detection: Tandem Mass Spec (MS-MS) @ (22°C)

Detector Info: SCIEX 3200 QTRAP®

Note:SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, Fusion-RP 4 x 2.0mm ID, 10/Pk Part No.: AJ0-7556
- Holder Part No.: KJ0-4282

Analyte Details

Analyte Detail not available

Acephate

Demeton-S-methyl sulfone

Parathion-methyl

Dicrotophos

Demeton-S-methyl

Dimethoate

Mevinphos

Dichlorvos

Phorate sulfoxide

Famphur

Naled

Azinphos-methyl

Malathion

Triazophos

Azinphos-ethyl

Tetrachlorvinphos

EPTC

Chlorfenvinphos

Parathion

Sulfotep

Diazinon

Fenthion

Coumaphos

Phorate

Pirimiphos-methyl

Pirimiphos-ethyl

Sulprofos

Chlorpyrifos

Tokuthion