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Screening of 535 Pesticides by QuEchERS and LC/MS/MS

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Application Detail (App ID: 20035)

Column: Synergi™ 2.5 µm Fusion-RP 100 Å, LC Column 50 x 2 mm, Ea

Part No:00B-4423-B0

Dimensions:50 x 2 mm ID

Elution Type:Gradient

Elution A:Water/Methanol (90:10) + 5 mM ammonium formate

Elution B:Methanol/Water (90:10) + 5 mM ammonium formate

Gradient Profile:

Step No.	Time (min)	Pct A	Pct B
1	0	100	0
2	1	100	0
3	15	0	100
4	18	0	100
5	18.05	100	0
6	20	100	0

Flow Rate:0.4 mL/min

Col. Temp: 40 °C

Detection: Tandem Mass Spec (MS-MS) @ (400°C)

Detector Info: SCIEX API 3200™

Note:Phenomenex SecurityGuard Guard Cartridge kit (P/N KJ0-4282) with C18 4 x 2.0 mm cartridge (P/N AJ0-4286)

Analyte Details

Analyte Detail not available

Aminopyralid

Glufosinate

Maleic hydrazide

Amitrol

Daminozide

Prohexadione

Ethylenthiourea

Clopyralid

Methamidophos

Acephate

Imazapyr

Mesotrione

Methomyl-oxime

Omethoate

Oxamyl-oxime

Atrazine-desethyl-2-hydroxy

Cyromazine

Aldoxycarb

Aldicarb-sulfoxide

Dinotefuran

Butocarboxim-sulfoxide

Sulcotrione

Butoxycarboxim

Quinmerac

6-Chlor-3-phenyl-pyridazin-4-ol

Nitenpyram

Flumetsulam

Methomyl

Oxamyl

Fluroxypyr

Flonicamid

Imazapic

Oxydemeton-methyl

Demeton-S-methyl sulfone

Thiamethoxam

Formetanate

Amidosulfuron

Dicyclanil

Atrazine-desisopropyl

Thiencarbazone-methyl

Monocrotophos

5-Hydroxy-imidacloprid

Imidacloprid-Olefin

Benazolin

Pymetrozine

Nicotine

Thiofanox-sulfoxide

2-Naphthyloxyacetic acid

Ethiofencarb-sulfone

Imazaquin

Propamocarb

Fenuron

5-Hydroxy-clethodim-sulfone

Diquat

Ethiofencarb-sulfoxide

Metsulfuron-methyl

Rimsulfuron

Simazine-2-hydroxy

Thifensulfuron-methyl

Dicrotophos

Trichlorfon

Clothianidin

Metamitron

Dioxacarb

Imidacloprid

Imazethapyr

Thiofanox-sulfone

Azimsulfuron

Chlorsulfuron

Diamidafos

Dimethoate

Ethidimuron

5-Hydroxythiabendazole

Chloridazon

Flucarbazone

3-Hydroxycarbofuran

Acetamiprid

Chlorthiamid

Vamidothion

Clethodim-imin-sulfone

Clethodim-imin-sulfoxide

Isocarbamid

Atrazine-desethyl

Cymoxanil

Diflufenzopyr

Flazasulfuron

Oxasulfuron

Propoxycarbazone

Carbendazim

Pyroxsulam

Dimetilan

Sulfometuron-methyl

Sulfosulfuron

Clethodim-sulfone

Clethodim-sulfoxide

Triasulfuron

Atrazine-2-hydroxy

Thiacloprid

Aldicarb

100

Foramsulfuron

101

Mevinphos

102

Tricyclazole

103

Tribenuron-methyl

104

3-Keto-carbofuran

105

Metoxuron

106

Halosulfuron-methyl

107

Iodosulfuron-methyl

108

Metolcarb

109

Desmethyl-pirimicarb

110

Ethametsulfuron-methyl

111

Paraoxon-methyl

112

Amicarbazone

113

Carbetamide

114

Flupyrsulfuron-methyl

115

Sebuthylazine-desethyl

116

Thiabendazole

117

Difenzoquat

118

Mesosulfuron-methyl

119

Monuron

120

Pyroquilon

121

Metribuzin

122

Oxadixyl

123

Fuberidazole

124

Penoxsulam

125

Quinoclamine

126

Bromacil

127

Carbofuran

128

Demeton-S-methyl

129

Dichlorvos

130

Phosphamidon

131

TEPP

132

Azamethiophos

133

Coumatetralyl

134

Cyanazine

135

Propoxur

136

Pyracarbolid

137

Thidiazuron

138

Tritosulfuron

139

Aminocarb

140

Chlordimeform

141

Metosulam

142

Simazine

143

Diclosulam

144

Hexazinone

145

Propazin-2-hydroxy

146

Bendiocarb

147

Desmethyl-formamido-pirimicarb

148

Terbacil

149

Thiophanate-methyl

150

Ofurace

151

Sulfentrazone

152

Tebuthiuron

153

Chlorimuron-ethyl

154

Ethoxysulfuron

155

Alloxydim

156

Carboxin

157

Prosulfuron

158

Terbuthylazine-desethyl

159

Carbaryl

160

Fenfuram

161

Imazamethabenz-methyl

162

Malaoxon

163

Terbuthylazine-2-hydroxy

164

Thiofanox

165

Warfarin

166

Monolinuron

167

DEET

168

Fluazifop

169

Methabenzthiazuron

170

Norflurazon-desmethyl

171

Ethiofencarb

172

Chlorotoluron

173

Fluometuron

174

Metobromuron

175

Clethodim

176

Phorate sulfoxide

177

Pirimicarb

178

Propham

179

Atrazine

180

Atrazine-d5

181

Isoprocarb

182

Simetryn

183

Triazoxide

184

Cycluron

185

Ethaboxam

186

Ethirimol

187

Cyanophos

188

Lenacil

189

Paraoxon

190

Phorate-sulfone

191

Propachlor

192

Thiodicarb

193

Diuron

194

Flutriafol

195

Isoproturon

196

Isoproturon-d6

197

Metazachlor

198

Quizalofop-P

199

Triflusulfuron-methyl

200

3,4,5-Trimethacarb

201

Buturon

202

Diphacinone

203

Forchlorfenuron

204

Metalaxyl-M

205

Azaconazole

206

Bensulfuron-methyl

207

Famphur

208

Dimethachlor

209

Heptenophos

210

Naled

211

Difenoxuron

212

Diphenamide

213

Isoxaflutole

214

Norflurazon

215

Thiophanate

216

Benfuresate

217

Benoxacor

218

Clomazone

219

Fomesafen

220

Methidathion

221

Phosmet

222

Secbumetone

223

Methacrifos

224

Methfuroxam

225

Prometon

226

Propanil

227

Acibenzolar-S-methyl

228

Desmedipham

229

Parathion-methyl

230

Pyrimethanil

231

Ametryn

232

Azinphos-methyl

233

Dimefuron

234

Fenobucarb

235

Methoprotryne

236

Phenmedipham

237

Propazine

238

Sebuthylazine

239

Fenpiclonil

240

Halofenozide

241

Linuron

242

Diethofencarb

243

Dimethenamide

244

Fluridone

245

Furalaxyl

246

Inabenfide

247

Methiocarb

248

Siduron

249

Terbumeton

250

Anilazine

251

Chlorbromuron

252

Chlorbufam

253

Ethiprole

254

Ethofumesate

255

Fenamidone

256

Nuarimol

257

Terbuthylazine

258

Chlorethoxyfos-oxon

259

Crotoxyphos

260

Fludioxonil

261

Mexacarbate

262

Molinate

263

Promecarb

264

Uniconazole

265

Azoxystrobin

266

Boscalid

267

Flurtamone

268

Propyzamide

269

Chlorophacinone

270

Paclobutrazol

271

Benthiavalicarb-isopropyl

272

Cyproconazole

273

Dimethomorph

274

Diphenylamine

275

Isoprothiolane

276

Isoxaben

277

Mandipropamid

278

Mepronil

279

Thiometon

280

Bromuconazole

281

Cumyluron

282

Cycloxydim

283

Daimuron

284

Flurprimidol

285

Flutolanil

286

Myclobutanil

287

Triadimefon

288

Triticonazole

289

Bensultap

290

Chloroxuron

291

Fenitrothion

292

Fenpropidin

293

Flamprop-M-methyl

294

Isofenphos-oxon

295

Mefenacet

296

Procymidone

297

Triadimenol

298

Triazamate

299

Trietazine

300

Acetochlor

301

Bifenazate

302

Flurochloridone

303

Isazofos

304

Mepanipyrim

305

Methoxyfenozide

306

Prometryne

307

Propetamphos

308

Pyridaphenthion

309

Triazophos

310

Alachlor

311

Fenhexamid

312

Fluquinconazole

313

Iprovalicarb

314

Pethoxamid

315

Prothioconazole desthio metabolite

316

Spirotetramat

317

Dichlofluanid

318

Ethoprop

319

Fenarimol

320

Flufenacet

321

Mecarbam

322

Metolachlor

323

Napropamide

324

Terbutryn

325

Azinphos-ethyl

326

Butafenacil

327

EPTC

328

Fluoxastrobin

329

Tetraconazole

330

Tralkoxydim

331

Epoxiconazole

332

Fenothiocarb

333

Pyrifenox

334

Sethoxydim

335

Cyazofamid

336

Diflubenzuron

337

Ethion monoxon

338

Fenamiphos

339

Fenbuconazole

340

Fenoxanil

341

Dimethametryn

342

Flusilazole

343

Isoxadifen-ethyl

344

Rotenone

345

Tetrachlorvinphos

346

Triflumuron

347

Aclonifen

348

Cyprodinil

349

Diclobutrazol

350

Dimoxystrobin

351

Fenoxycarb

352

Kresoxim-methyl

353

Neburon

354

Parathion

355

Quinalphos

356

Benomyl

357

Bensulide

358

Bupirimate

359

Carfentrazone-ethyl

360

Clodinafop-propargyl

361

Etrimfos

362

Fipronil

363

Fluthiacet-methyl

364

Fluxofenim

365

Imazalil

366

Penconazole

367

Phenthoate

368

Picoxystrobin

369

Prothioconazole

370

Spiroxamine

371

Tebuconazole

372

Tebufenozide

373

Alanycarb

374

Chinomethionate

375

Edifenphos

376

Etobenzanid

377

Fenthion

378

Phorate

379

Propiconazole

380

Sulfotep

381

Tolylfluanid

382

Anilofos

383

Beflubutamid

384

Benalaxyl

385

Chlorfenvinphos

386

Cyanofenphos

387

Diazinon

388

Flamprop-M-isopropyl

389

Fonofos

390

Malathion

391

Zoxamide

392

Carpropamid

393

Hexaconazole

394

Mefenpyr-diethyl

395

Orbencarb

396

Pyraflufen-ethyl

397

Tris-(1,3-dichloro-isopropyl)-phosphate

398

Coumaphos

399

Difenacoum

400

Disulfoton

401

Metconazole

402

Pebulate

403

Prochloraz

404

Thiobencarb

405

Tolclofos-methyl

406

Triphenyl phosphate

407

Bitertanol

408

Clofentezine

409

Famoxadone

410

Isoxathion

411

Oxadiargyl

412

Phosalone

413

Pirimiphos-methyl

414

Pyraclofos

415

Pyraclostrobin

416

Benzoximate

417

Chlorpyrifos-methyl

418

Cycloate

419

Cyflufenamid

420

Diniconazole

421

Metrafenone

422

Pencycuron

423

Phoxim

424

Pyrazophos

425

Cadusafos

426

Dimepiperate

427

Isofenphos

428

Bifenox

429

Dialifos

430

Di-allate

431

Difenoconazole

432

Haloxyfop-P-methyl

433

Iprodione

434

EPN

435

Ipconazole

436

Piperophos

437

Prosulfocarb

438

Butylate

439

Cyhalofop-butyl

440

Dodine

441

MCPA-butotyl

442

Trifloxystrobin

443

Chlormephos

444

Clomeprop

445

Indoxacarb

446

Profenofos

447

Triflumizole

448

Cinidon-ethyl

449

Esprocarb

450

Fenoxaprop-P-ethyl

451

Fluoroglycofene-ethyl

452

Benfuracarb

453

Brodifacoum

454

Diclofop-methyl

455

Dithiopyr

456

Haloxyfop-etotyl

457

Hexaflumuron

458

Quizalofop-ethyl

459

Tebufenpyrad

460

Terbufos

461

Fluazifop butyl

462

Furathiocarb

463

Propaquizafop

464

Tebupirimfos

465

Teflubenzuron

466

Tetramethrin

467

Bioallethrin

468

Bromophos

469

Buprofezin

470

Cloquintocet-mexyl

471

Imibenconazole

472

Oxadiazon

473

Oxyfluorfen

474

Piperonyl butoxide

475

Dichlofenthion

476

Novaluron

477

Picolinafen

478

Pirimiphos-ethyl

479

Pyriproxyfen

480

Quinoxyfen

481

Triallate

482

Aramite

483

Dioxathion

484

Ethion

485

Lactofen

486

Dodemorph

487

Hexythiazox

488

Pendimethalin

489

Sulprofos

490

Temephos

491

Hydramethylnon

492

Pyrethrin I

493

Butralin

494

Chlorthiophos

495

Fentin

496

Flucycloxuron

497

Fluroxypyr-meptyl

498

Lufenuron

499

Propargite

500

Spiromesifen

501

Aspon

502

Fenpropathrin

503

Flucythrinate

504

Flufenoxuron

505

Spirodiclofen

506

Cyfluthrin

507

Fenpyroximate

508

Spinosyn A

509

Cypermethrin

510

Fenazaquin

511

Fenpropimorph

512

Chlorfluazuron

513

Deltamethrin

514

lambda-Cyhalothrin

515

Pyridaben

516

Cyphenothrin

517

Esfenvalerate

518

Fenvalerate

519

Prothiophos

520

Spinosyn D

521

Bioresmethrin

522

Resmethrin

523

Spinetoram A

524

MCPA-2-Ethylhexylester

525

Pyridate

526

tau-Fluvalinate

527

Bifenthrin

528

Carbosulfan

529

Permethrin

530

Tridemorph

531

Etofenprox

532

Spinetoram B

533

Moxidectin

534

Halfenprox

535

Pyridalyl