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EPA 552.2 by GC/ECD on ZB-CLPesticides-2 (Helium Gas)

Application Detail (App ID: 22669)

Part No:7HM-G029-11
Phase:Proprietary Pesticides Phase
Dimensions:30 meters x 0.32 mm x 0.25 µm
Oven Profile:35 °C for 4 min to 250 °C @ 15 °C/min, hold 5 min
Carrier Gas:Constant Flow Helium, 25 cm/sec
Injection:Splitless :1 1 µL @ 250°C
Detection: Electron Capture (ECD) (300°C)
Note:1.0 µL pulsed splitless @ 25 psi for 0.75 minutes. Analytes are various concentrations in ethyl acetate:
1. Methyl chloroacetate (1500 ng/mL)
2. Methyl bromoacetate (1000 ng/mL)
3. Methyl dichloroacetate (1500 ng/mL)
4. Dalapon methyl ester (1000 ng/mL)
5. Methyl trichloroacetate (500 ng/mL)
6. 1,2,3-Trichloropropane (4000 ng/mL)
7. Methyl bromochloroacetate (1000 ng/mL)
8. Methyl bromodichloroacetate (1000 ng/mL)
9. Methyl dibromoacetate (500 ng/mL)
10. Methyl chlorodibromoacetate (2500 ng/mL)
11. 2,3 dibromopropionate (2000 ng/mL)
12. Methyl tribromoacetate (5000 ng/mL)

Y-Connector: AG0-4717 (Fused Quartz)
Guard Column: 7AM-G000-00-GZ0 (5 m Z-Guard™)
Liner: AG0-8499 (Single Taper with Wool at Bottom)
Septum: AG0-4696 (PhenoRed™-400)
Inlet Seal: AG0-8620 (Gold-Plated Easy Seal™)

Analyte Details

Analyte Detail not available

1
Methyl monochloroacetate
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2
Methyl monobromoacetate
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3
Methyl dichloroacetate
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4
Dalapon methyl ester
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5
Methyl trichloroacetate
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6
1,2,3-Trichloropropane (IS)
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7
Methyl bromo(chloro)acetate
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8
Methyl bromodichloroacetate
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9
Methyl dibromoacetate
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10
Methyl chlorodibromoacetate
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11
Methyl 2,3-dibromopropionate (SS)
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12
Methyl tribromoacetate
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