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NDMA and NDEA by GC/MS on a ZB-624Plus (Valsartan Tablet #2)

Application Detail (App ID: 25328)

Part No:7HG-G040-27
Phase:Proprietary Pesticides Phase
Dimensions:30 meters x 0.25 mm x 1.4 µm
Oven Profile:60°C for 1 min to 240°C @ 20°C/min 240°C for 1 min
Carrier Gas:Constant Flow Helium, 36.1 cm/sec
Injection:Split 10:1 1 µL @ 150°C
Detection: GC/MS (250°C)
Note:500 mg Valsartan tablet (#2) analyzed and found to contain 10 ppb NDMA and 139 ppb NDEA Tablet was crushed and mixed in 1 mL of DMSO in a 20 mL headspace vial.

Analyte Details

Analyte Detail not available

1
NDMA
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2
NDEA
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