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Identification and Quantification of Designer Drugs in Urine by LC-MS/MS

Application Detail (App ID: 25865)

Part No:00F-4462-Y0
Dimensions:150 x 3 mm ID
Elution Type:Gradient
Elution A:Ammonium formate in water
Elution B:Acetonitrile
Gradient Profile:
Step No. Time (min) Pct A Pct B
1 0 95 5
2 6 5 95
3 6.2 5 95
4 8 95 5

Flow Rate:0.5 mL/min
Col. Temp: 50 °C
Detection: LC/MS/MS @ (0°C)
Note:To 20 µL urine, add 50 µL internal standard (D5-PCP in acetonitrile). Vortex then centrifuge for 10 min at 15,000 rpm.

Dilute supernatant with 930 µL Mobile Phase A. Mix and transfer to an autosampler vial for injection.

Analyte Details

Analyte Detail not available

1
Dehydronorketamine
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2
Norketamine
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3
Ketamine
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4
Methoxetamine
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5
3-MeO-PCE
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6
3-MeO-PCP
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