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LC-MS/MS Pesticides (Metolachlor) - NY Filter in Chili Exacts for the comparison of with/without Filter Vial

Application Detail (App ID: 26529)

Part No:00F-4784-Y0
Dimensions:150 x 3 mm ID
Elution Type:Gradient
Elution A:0.1% Formic Acid and 10mM Ammonium Acetate in water
Elution B:0.5% Formic Acid in Methanol
Gradient Profile:
Step No. Time (min) Pct A Pct B
1 0 95 5
2 0.1 95 5
3 0.5 40 60
4 3.5 25 75
5 8 15 85
6 10.5 5 95
7 12 5 95
8 12.1 95 5
9 18 95 5

Flow Rate:0.4 mL/min
Col. Temp: 20 °C
Detection: LC/MS/MS @ (0°C)
Note:a) Prepared 1mg/mL Metolachlor solutions with other 17 pesticide standards
b) Take sample to prepare a 10x Diluted mixture by placing 100uL of the existing mix into a 900uL of a 1:2 Water:Acetonitrile mix.
c) Place 30uL of the 10x diluted mixture into 270 uL of the chili powder supernatant.
d) Place 450uL of sample from step c) into the filter vial for final analysis.

Analyte Details

Analyte Detail not available

1
Metolachlor
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2
Metolachlor
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