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USP Rivaroxaban Assay and Organic Impurities - Standard Solution Assay run on Agilent® 1260

Application Detail (App ID: 28023)

Part No:00F-4784-Y0
Dimensions:150 x 3 mm ID
Elution Type:Gradient
Elution A:Buffer(10mM potassium dihydrogen phosphate, 5.3mM sodium hexanesulfonate, 3.77mM phosphoric acid in water)/Methanol (95:5)
Elution B:ACN
Gradient Profile:
Step No. Time (min) Pct A Pct B
1 0 98 2
2 1.22 98 2
3 6.36 84 16
4 20.93 64 36
5 31.22 20 80
6 31.3 98 2
7 38.3 98 2

Flow Rate:1 mL/min
Col. Temp: 60 °C
Detection: LC/UV (DAD, PDA) @ 250.0000000000 nm (nanometers) (0°C)
Note:Solution B: 5.3mM sodium hexane sulfonate, 3.77mM phosphoric acid in water
Diluent: Acetonitrile and solution B (40:60)
Standard solution: 0.5 mg/mL of USP Rivaroxaban RS in Diluent​
peak no. 1
analyte name: standard solution
RT (min): 15.609
conc.: 0.5mg/mL

Analyte Details

Analyte Detail not available

1
Rivaroxaban
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