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Quantification of Carbamates Fungicides in Beverage by LC/MS/MS

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Sample Preparation Details

Part Number :8B-S100-TBJ

Description :Strata-X 33 µm Polymeric Reversed Phase, 30 mg / 3 mL, Tubes, 50/Pk

Condition 1 :1 mL Methanol

Condition 2 :1 mL 25 mM Ammonium acetete pH 5.5

Load :Load 1.40 mL Sample diluted in pretreated sample

Wash 1 :1 mL 25 mM Ammonium acetete pH 5.5

Wash 2 :1 mL Methanol/Water (15:85)

Dry :2 min at 10mm Hg

Elution 1 :0.5 mL 5% Formic acid in Methanol

Evaporate: :Evaporate to dryness

Reconstitute :1 mL Initial mobile phase

Application Detail (App ID: 20025)

Column: Gemini® 3 µm C18 110 Å, LC Column 50 x 2 mm, Ea

Part No:00B-4439-B0

Dimensions:50 x 2 mm ID

Elution Type:Gradient

Elution A:5mM ammonium formate

Elution B:5mM ammonium formate in acetonitrile

Gradient Profile:

Step No.	Time (min)	Pct A	Pct B
1	0	85	15
2	2.5	5	95
3	4	5	95
4	4.01	85	15
5	8	85	15

Flow Rate:0.5 mL/min

Col. Temp: 28 °C

Detection: Tandem Mass Spec (MS-MS) @ (22°C)

Detector Info: 3200 QTRAP

Note:SecurityGuard™ Guard Cartridge System extends column lifetime.
- SecurityGuard Cartridges, Gemini C18 4 x 2.0mm ID, 10/Pk Part No.: AJ0-7596
- Holder Part No.: KJ0-4282

Analyte Details

Analyte Detail not available

Aldicarb-sulfone

Methomyl

3-Hydroxycarbofuran

Oxamyl

Aldicarb

Carbofuran

Carbofuran-d3

Methiocarb