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Cannabinoids from Food using roQ and ZB-5MSplus

Application Detail (App ID: 23229)

Part No:7HG-G030-11
Phase:
Dimensions:30 meters x 0.25 mm x 0.25 µm
Oven Profile:100 ºC for 1 min to 320 ºC at 50 ºC/min hold for 2 min.
Carrier Gas:Constant Flow Helium, 1.5 mL/min
Injection:Splitless :1 1 µL @ 250°C
Detection: Mass Selective (MSD) (320°C)
Note:Sample preparation: Combine 1 g of chocolate brownie with 10 mL of water in a 50 mL centrifuge tube. Shake using mechanical shaker until dissolved. Add EN15662 roQ quechers extraction salt packet (KS0-8909) and 10 mL of acetonitrile. Shake tube for 3 min using mechanical shaker. Centrifuge at 2700 rpm for 5 min. Transfer 1 mL of supernatant to an autosampler vial for GC/MS analysis.

Brownie contained 1 µg/g cannabinoids.

Sim mode: CBD (231.1, 246.1, 314.2), THC (299.1, 231.1, 310.2), CBN (295.1, 238.1, 310.2)

Analyte Details

Analyte Detail not available

1
Cannabidiol
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2
delta-9-Tetrahydrocannabinol
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3
Cannabinol
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